Bromination-Carbon Reduction Method for the Determination of Oxygen in Metals

Maurice Codell; George Norwitz; Silve Kallmann

doi:10.1520/STP41198S

SYMPOSIA PAPER Published: 01 January 1958

STP41198S

Bromination-Carbon Reduction Method for the Determination of Oxygen in Metals

Source

The principles of the bromination-carbon reduction method for determining oxygen in metals are discussed. A simplified apparatus and an improved procedure are described and the effect of certain variables is considered. The optimum temperature for the bromination reaction is approximately 900 C. At temperatures considerably less or greater, the reaction is slower. The use of bromine free from organic compounds is desirable. Graphite, platinum, or gold boats may be used. The method has been applied to the determination of oxygen in titanium, zirconium, chromium, vanadium, steels, and other metals. It is not applicable to steels containing oxide inclusions.

Author Information

Codell, Maurice

Pitman-Dunn Laboratories., Philadelphia, Pa

Norwitz, George

Pitman-Dunn Laboratories., Philadelphia, Pa

Kallmann, Silve

Ledoux and Co., Teaneck, N. J.

Shipping & Handling

Domestic Shipping

Domestic orders are delivered via United Parcel Service (UPS) or United States Postal Service (USPS). Transit times average 3 to 5 business days. Please be aware that UPS will not deliver packages to Post Office Boxes.

Domestic Rush Orders

Please Contact Us.

International Standard Shipping

International orders are delivered via courier post services which can be either a postal service, courier service, or a combination of both. Standard Service is untraceable. Please allow 4-7 weeks for delivery.

International Expedited Shipping

Please Contact Us.

Please be aware that carriers will not deliver packages to Post Office Boxes. Because of the variability of customs processes and procedures in different countries, ASTM International cannot guarantee transit times to international destinations. Customs duty and taxes are the responsibility of the consignee.

Shipping & Handling charges follow the rate schedule, below:

Order Total	Shipping & Handling Fee (US Domestic)
Up to $50.00	$18.72
$50.01 to $100.00	$20.80
$100.01 to $150.00	$29.52
$150.01 to $250.00	$39.09
$250.01 to $500.00	$56.25
$500.01 to $750.00	$76.42
$750.01 to $1000.00	$93.15
$1000.01 to $1500.00	$121.27
$1500.01 to $2500.00	$158.38
$2500.01 to $4999.00	$209.04
$5000.00 to higher	FREE

Order Total	Shipping & Handling Fee (International)
Up to $50.00	$68.72
$50.01 to $100.00	$70.80
$100.01 to $150.00	$79.52
$150.01 to $250.00	$89.09
$250.01 to $500.00	$106.25
$500.01 to $750.00	$126.42
$750.01 to $1000.00	$143.15
$1000.01 to $1500.00	$171.27
$1500.01 to $2500.00	$208.38
$2500.01 to $4999.00	$259.04
$5000.00 to higher	FREE

Shipping and Handling charges are approximate. Additional charges may be incurred if your order requires multiple shipments. This does not apply to complete sets and sections.

Reprints and Permissions

Reprints and copyright permissions can be requested through the
Copyright Clearance Center

Details

Developed by Committee: E01

Pages: 33–40

DOI: 10.1520/STP41198S

ISBN-EB: 978-0-8031-5947-1

ISBN-13: 978-0-8031-6101-6

Bromination-Carbon Reduction Method for the Determination of Oxygen in Metals

Author Information

Related

Reprints and Permissions

Details