Determination of Radionuclides in Biological Fluids Using a High Resolution ICP-MS in Low Resolution Mode

CJ Pickford; J Haines; R Heam; J McAughey

doi:10.1520/STP15731S

SYMPOSIA PAPER Published: 01 January 1998

STP15731S

Determination of Radionuclides in Biological Fluids Using a High Resolution ICP-MS in Low Resolution Mode

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High Resolution (HR) ICP-MS in low resolution mode was used with ultrasonic nebulization to determine long-lived radionuclides and surrogates in human body fluid samples. Although very sensitive, achieving LODs less than 0.1 fg/mL for ²⁴⁴Pu, a number of molecular ion interferences have been encountered from commonly-occurring species which limit sensitivity and require the development of specialized sample preparation routes.

Author Information

Pickford, CJ

AEA Technology/ Analytical Services, Didcot, Oxfordshire, England

Haines, J

AEA Technology/ Analytical Services, Didcot, Oxfordshire, England

Heam, R

AEA Technology/ Analytical Services, Didcot, Oxfordshire, England

McAughey, J

AEA Technology, Didcot, Oxfordshire, England

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Details

Developed by Committee: C26

Pages: 111–119

DOI: 10.1520/STP15731S

ISBN-EB: 978-0-8031-5390-5

ISBN-13: 978-0-8031-2034-1

Determination of Radionuclides in Biological Fluids Using a High Resolution ICP-MS in Low Resolution Mode

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