Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry
Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning CalorimetryE1356-25ASTM|E1356-25|en-USStandard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning CalorimetryStandardE1356 Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry>newBOS Vol. 14.01 Committee E37
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Significance and Use
5.1 DSC provides a rapid test method for determining changes in specific heat capacity in a homogeneous material. The glass transition is manifested as a step change in specific heat capacity. For amorphous and semicrystalline materials the determination of the glass transition temperature may lead to important information about their thermal history, processing conditions, stability, progress of chemical reactions, and mechanical and electrical behavior.
5.2 This test method is useful for research, quality control, and specification acceptance.
Scope
1.1 This test method covers the assignment of the glass transition temperatures of materials using differential scanning calorimetry (DSC) or differential thermal analysis (DTA).
1.2 This test method is applicable to amorphous materials or to partially crystalline materials containing amorphous regions, that are stable and do not undergo decomposition or sublimation in the glass transition region.
1.3 The normal operating temperature range is from −120 °C to 500 °C. The temperature range may be extended, depending upon the instrumentation used.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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