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Standard
Withdrawn, No replacement
Last Updated: May 17, 2018
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ASTM E963-95(2017)
Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte (Withdrawn 2018)
Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte (Withdrawn 2018)
E0963-95R17
ASTM|E0963-95R17|en-US
Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte (Withdrawn 2018)
Standard
E963 Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte (Withdrawn 2018)>
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Significance and Use
3.1 This practice can be used to extract carbides, borides, TCP and GCP phases, which can then be qualitatively or quantitatively analyzed by X-ray diffraction or microanalysis.2
3.2 Careful control of parameters is necessary for reproducible quantitative results. Within a given laboratory, such results can be obtained routinely; however, caution must be exercised when comparing quantitative results from different laboratories.3
3.3 Comparable qualitative results can be obtained routinely among different laboratories using this procedure.3
Scope
1.1 This practice covers a procedure for the isolation of carbides, borides, TCP (topologically close-packed), and GCP (geometrically close-packed) phases (Note 1) in nickel and nickel-iron base gamma prime strengthened alloys. Contamination of the extracted residue by coarse matrix (gamma) or gamma prime particles, or both, reflects the condition of the alloy rather than the techniques mentioned in this procedure.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See 4.3.2.1 and 5.1.1.)
Note 1: Ni3 Ti (eta phase) has been found to be soluble in the electrolyte for some alloys. FIG. 1 Schematic Diagram of Extraction Cell 
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.