Standard Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP) and Atomic Absorption (AA)
Standard Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP) and Atomic Absorption (AA)C1301-95R09E01ASTM|C1301-95R09E01|en-USStandard Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP) and Atomic Absorption (AA)StandardC1301 Standard Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP) and Atomic Absorption (AA)>newBOS Vol. 04.01 Committee C07
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Significance and Use
The presence and concentration of elements in lime and limestone is important in determining product quality and its suitability for various uses. This test method provides a means of measuring the major and trace element concentration in lime and limestone.
Scope
1.1 The following test method covers the use of inductively coupled plasma-atomic emission spectroscopy (ICP) and atomic absorption spectroscopy (AA) in the analysis of major and trace elements in limestone and lime (calcined limestone).
1.2 Table 1 lists some of the elements that can be analyzed by this test method and the preferred wavelengths. Also see U.S. EPA Methods 200.7 and 200.9.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
TABLE 1 Elements and Some Suggested WavelengthsA
Major Elements
ICP Wavelength, nm
AA Wavelength, nm
Calcium
317.933 (315.887)B
422.7
Magnesium
279.079 (285.213)
285.2
Silicon
251.611 (288.160)
251.6
Aluminum
308.215 (309.271)
309.3
Iron
259.940
248.3
Manganese
257.610
279.5
Sodium
588.995 (589.59)
589.0
Potassium
766.491
766.5
Phosphorus
214.914 (213.618)
...C
Strontium
421.552
460.7
Trace Elements
ICP Wavelength, nm
AA Wavelength, nm
Antimony
206.833
217.6
Arsenic
193.696
193.7
Barium
455.403 (493.409)
553.6
Beryllium
313.042
234.9
Boron
249.773
249.8
Cadmium
226.502 (228.80)
228.8
Chromium
267.716 (205.552)
357.9
Cobalt
228.616
240.7 (242.5)
Copper
324.754
324.8
Lead
220.353
217.0 (283.3)
Molybdenum
202.030 (203.844)
313.3
Nickel
231.604 (221.647)
232.0
Selenium
196.090
196.0
Silver
328.068
328.1
Sulfur
180.731 (180.669)
...C
Thallium
190.864
276.8
Tin
189.989
235.5 (286.3)
Vanadium
292.402
318.4
Zinc
213.856 (202.551)
213.9
A The suggested wavelengths may vary for your particular instrument.
B Numbers in parentheses are alternate wavelengths.
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