Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride
Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium HexafluorideC0761-04ASTM|C0761-04|en-USStandard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium HexafluorideStandardC761 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride>newBOS Vol. 12.01 Committee C26
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Scope
1.1 These test methods cover procedures for subsampling and for chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of uranium hexafluoride (UF6). Most of these test methods are in routine use to determine conformance to UF6 specifications in the Enrichment and Conversion Facilities.
1.2 The analytical procedures in this document appear in the following order:
Note 1—Subcommittee C26.05 will confer with C26.02 concerning the renumbered section in Test Methods C761 to determine how concerns with renumbering these sections, as analytical methods are replaced with stand-alone analytical methods, are best addressed in subsequent publications.
Sections
Subsampling of Uranium Hexafluoride
7 - 10
Gravimetric Determination of Uranium
11 - 19
Titrimetric Determination of Uranium
20
Preparation of High-Purity U3O 8
21
Isotopic Analysis
22
Isotopic Analysis by Double-Standard Mass-Spectrometer Method
23 - 29
Determination of Hydrocarbons, Chlorocarbons, and Partially Substituted Halohydrocarbons
29-36
Atomic Absorption Determination of Antimony
36
Spectrophotometric Determination of Bromine
37
Titrimetric Determination of Chlorine
38-44
Determination of Silicon and Phosphorus
45-51
Determination of Boron and Silicon
52-59
Determination of Ruthenium
60
Determination of Titanium and Vanadium
61
Spectrographic Determination of Metallic Impurities
62
Determination of Tungsten
63
Determination of Thorium and Rare Earths
64-69
Determination of Molybdenum
70
Atomic Absorption Determination of Metallic Impurities
71-76
Impurity Determination by Spark-Source Mass Spectrography
77
Determination of Boron-Equivalent Neutron Cross Section
78
Determination of Uranium-233 Abundance by Thermal Ionization Mass Spectrometry
79
Determination of Uranium-232 by Alpha Spectrometry
80-86
Determination of Fission Product Activity
87
Determination of Plutonium by Ion Exchange and Alpha Counting
88-92
Determination of Plutonium by Extraction and Alpha Counting
93-100
Determination of Neptunium by Extraction and Alpha Counting
101-108
Atomic Absorption Determination of Chromium Soluble In Uranium Hexafluoride
109-115
Atomic Absorption Determination of Chromium Insoluble In Uranium Hexafluoride
116-122
Determination of Technetium-99 In Uranium Hexafluoride
123-131
Method for the Determiation of Gamma-Energy Emission Rate from Fission Products in Uranium Hexafluoride
132
Determination of Metallic Impurities by ICP-AES
133-142
Determination of Molybdenum, Niobium, Tantalum, Titanium, and Tungsten by ICP-AES
143-152
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safeguard and safety consideration statements, see Section 6.)
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